Pwodwi

2,3-Lutidin

Pwodwi Entwodiksyon

2,3-Lutidine Enfòmasyon de baz

Non pwodwi:	2,3-Lutidin
Sinonim:	2,3-DIMETHYLPYRIDINE(2,3-LUTIDINE);a,b-Dimethylpyridine;2,3-Lutidine (8CI);Pyridine, 2,3-dimethyl- (9CI) );2,3-Lutidin, 98+% 100ML;2,3- deMethylpyridine;2,3-Lutidin 99%;LUT
CAS:	583-61-9
MF:	C7H9N
mw:	107.15
EINECS:	209-514-1
Kategori pwodwi:	Byochimi;Reyaktif pou sentèz oligosakarid;Pyridin dérivés;Konpoze eterosiklik;bc0001
Mol File:	583-61-9.mol

2, 3-Lutidine Pwopriyete Chimik

Pwen k ap fonn	-15 degre (lit.)
Pwen bouyi	162-163 degre (lit.)
dansite	0.945 g/mL nan 25 degre (lit.)
endèks refraktif	n20% 2FD 1.508 (lit.)
Fp	122 degre F
tanperati depo.	Atmosfè inaktif, Tanperati chanm
pka	6.57 (nan 25 degre)
fòm	Likid
koulè	Klè san koulè a yon ti kras jòn
Solibilite dlo	95 g/L (26 ºC)
retni	106418
InChiKey	HPYNZHMRTWQTB-UHFFFAOYSA-N
SOURI	CC{{0}C (N=CC=C1)C
Boutèy demè	1.638 (est)
Referans baz done CAS	583-61-9(Referans baz done CAS)
Referans Chimi NIST	Piridin, 2,3-dimetil-(583-61-9)
Sistèm Rejis Sibstans EPA	2,3-dimetilpiridin (583-61-9)

Enfòmasyon sou Sekirite

Kòd danje	Xn, F, Xi
Deklarasyon Risk	10-22-37/38-41-20/21/22-36/37/38
Deklarasyon Sekirite	16-26-39-36/37-36/37/39
RIDADÈ	UN 1993 3/PG 3
WGK Almay	3
tSCA	Wi
HazardClass	6.1
Pake Group	II
Kòd HS	29333990

Enfòmasyon MSDS

Founisè	Lang
2,3-dimetilpiridin	angle
Sigmaaldrich	angle
ATRAVÈ	angle
ALFA	angle

2, 3- Itilizasyon ak sentèz lutidin

Deskripsyon	2,3-Lutidine fè pati gwoup piridin dérivés e li se yon reyaktif òganik ki disponib nan komès ki itilize kòm yon entèmedyè nan sentèz òganik ak kòm yon ajan ki relye asid. Li se tou itilize kòm yon aditif manje pou rezon arom.
Pwopriyete chimik	klè san koulè likid yon ti kras jòn
Itilizasyon	2,3-Lutidine se yon entèmedyè lansoprazole. Li se itilize kòm entèmedyè pharmaceutique.
Definisyon	LOTUS: 2,3-Lutidine se yon pwodwi natirèl yo jwenn nan Nicotiana tabacum ak done ki disponib.
Referans sentèz (yo)	Journal of Organic Chemistry, 66, p. 53, 2001DOI:10.1021/jo000724t
Metòd pou pirifye	Vapè distile li nan yon solisyon ki gen apeprè 1.2 ekivalan 20% H2SO4, jiskaske ka 10% nan baz la te pote sou ak enpurte ki pa debaz yo. Lè sa a, solisyon asid la fè alkalin, epi baz la separe, seche sou NaOH oswa BaO, ak fraksyon distile. Lutidin distile a konvèti nan konplèks ure li yo pa brase 100g ak 40g ure nan 75mL H2O, refwadisman a 5o, filtraj nan ponp lan, epi lave ak 75mL H2O. Konplèks la, ki fonn nan 300mL H2O, se vapè distile jiskaske distile a pa bay okenn twoub ak yon ti kras NaOH solid. Lè sa a, distile a trete ak depase NaOH solid, epi yo retire kouch siperyè a: Lè sa a, kouch akeuz la ekstrè ak etè dyetil. Kouch anwo a ak ekstrè etè a konbine, seche (K2CO3), epi distile atravè yon kolòn kout. Pirifikasyon final la se pa kristalizasyon fraksyon lè l sèvi avèk konjelasyon pasyèl. Picrate a kristalize nan EtOH ak m 187-188o. [Kyte et al. J Chem Soc 4454 1960, Beilstein 20 H 243, 20 II 159, 20 III/IV 2765, 20/6 V 15.]

2, 3-Pwodwi Preparasyon Lutidine ak matyè premyè

Matyè premyè

2,3,4-trimethylpyridine-->Pyridine, 1,2,3,4-tetrahydro-5,6-dimethyl--->(2-Methylpyridin-3-yl)methyl acetate-->Ethanone, 1-(1-methyl-3-piperidinyl)- (9CI)-->2,3,6-TRIMETHYLPYRIDINE-->(2-METHYL-PYRIDIN-3-YL)-METHANOL-->3-Ethylpyridine-->2-metilnicotinate etil

Preparasyon pwodwi yo

2-Chloromethyl-3-methyl-4-(2,2,2-trifluoroethoxy)pyridine hydrochloride-->3-METHYL-2-PYRIDINECARBOXALDEHYDE-->2-HYDROXYMETHYL-3-METHYLPYRIDINE-->2,3-DIMETHYL-PYRIDIN-4-YLAMINE-->2-Chloromethyl-3-methyl-4-(3-methoxypropoxy)pyridine hydrochloride-->4-Chloro-2,3-dimethylpyridine 1-oxide-->Lansoprazole-->2-HYDROXYMETHYL-4-METHOXYPROPOXY-3-METHYLPYRIDINE-->4-Nitro-2,3-lutidine-N-oxide-->2,3-Dimethylpyridine-N-oxide-->2,6-Lutidine-->Piridin

Baj popilè: 2,3-lutidine, Lachin 2,3-lutidine manifaktirè, founisè, faktori

On: 3,5-Lutidin

Pwochen: 4-Syanopiridin

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